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Prof. Mostafa Yassin Mohamed Yassin Nassar :: Publications: |
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| Title: | Novel isatinoxime molybdenum and chromium complexes: Synthesis,
spectroscopic, and thermal characterization |
| Authors: | Mostafa Y. Nassar , Attia S. Attia, Shaymaa Adawy , M.F. El-Shahat |
| Year: | 2015 |
| Keywords: | Not Available |
| Journal: | Journal of Molecular Structure |
| Volume: | 1026 |
| Issue: | Not Available |
| Pages: | 88–92 |
| Publisher: | Elsevier |
| Local/International: | International |
| Paper Link: | |
| Full paper | Mostafa Yassin Mohamed Yassin Nassar_Novel isatinoxime molybdenum and chromium complexes Synthesis.pdf |
| Supplementary materials | Not Available |
| Abstract: |
Reactions of molybdenum and chromium hexacarbonyls with isatin-3-oxime (H2L) in THF were carried out under sun light or according to the traditional thermal reflux synthetic routes. Di-l-oxo bimolybdenum complex, [Mo(H2L)(THF)(O)2]2 was successfully synthesized under the reflux conditions. However, the dichromium oxo complex, [Cr(H2L)(O)2]2 was prepared using the sun light route. The prepared complexes were characterized using elemental analysis, IR, mass spectrometry, UV–Vis spectra, thermal analysis, and magnetic measurements. |
