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Prof. Mostafa Yassin Mohamed Yassin Nassar :: Publications:
Novel isatinoxime molybdenum and chromium complexes: Synthesis, spectroscopic, and thermal characterization
|Authors:||Mostafa Y. Nassar , Attia S. Attia, Shaymaa Adawy , M.F. El-Shahat|
|Journal:||Journal of Molecular Structure|
|Full paper||Mostafa Yassin Mohamed Yassin Nassar_Novel isatinoxime molybdenum and chromium complexes Synthesis.pdf|
|Supplementary materials||Not Available|
Reactions of molybdenum and chromium hexacarbonyls with isatin-3-oxime (H2L) in THF were carried out under sun light or according to the traditional thermal reflux synthetic routes. Di-l-oxo bimolybdenum complex, [Mo(H2L)(THF)(O)2]2 was successfully synthesized under the reflux conditions. However, the dichromium oxo complex, [Cr(H2L)(O)2]2 was prepared using the sun light route. The prepared complexes were characterized using elemental analysis, IR, mass spectrometry, UV–Vis spectra, thermal analysis, and magnetic measurements.