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Dr. Mostafa Yassin Mohamed Yassin Nassar :: Publications:

Title:
Novel isatinoxime molybdenum and chromium complexes: Synthesis, spectroscopic, and thermal characterization
Authors: Mostafa Y. Nassar , Attia S. Attia, Shaymaa Adawy , M.F. El-Shahat
Year: 2015
Keywords: Not Available
Journal: Journal of Molecular Structure
Volume: 1026
Issue: Not Available
Pages: 88–92
Publisher: Elsevier
Local/International: International
Paper Link:
Full paper Mostafa Yassin Mohamed Yassin Nassar_Novel isatinoxime molybdenum and chromium complexes Synthesis.pdf
Supplementary materials Not Available
Abstract:

Reactions of molybdenum and chromium hexacarbonyls with isatin-3-oxime (H2L) in THF were carried out under sun light or according to the traditional thermal reflux synthetic routes. Di-l-oxo bimolybdenum complex, [Mo(H2L)(THF)(O)2]2 was successfully synthesized under the reflux conditions. However, the dichromium oxo complex, [Cr(H2L)(O)2]2 was prepared using the sun light route. The prepared complexes were characterized using elemental analysis, IR, mass spectrometry, UV–Vis spectra, thermal analysis, and magnetic measurements.

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